微波技术在锂离子电池正极材料高效回收再利用中的研究进展

孙静; 江镇宇; 于冠群; 贾平山; 王文龙

doi:10.12030/j.cjee.202009024

[1]

DENG S J, ZHU H, WANG G Z, et al. Boosting fast energy storage by synergistic engineering of carbon and deficiency[J]. Nature Communications, 2020, 11(1): 1-11. doi: 10.1038/s41467-019-13993-7

[2]

ZHANG L S, WANG H, WANG L Z, et al. High electrochemical performance of lithium-rich Li_1.2Mn_0.54Ni_xCo_yO₂ cathode materials for lithium-ion batteries[J]. Materials Letters, 2016, 185: 100-103. doi: 10.1016/j.matlet.2016.08.118

[3]

BHATLU M L D, BHAUMIK M, SUKANYA K. Energy management by using lithium-ion batteries, piezo materials, sensors and renewal energy system in the daily life: A review[J]. Journal of Critical Reviews, 2020, 7(7): 798-801. doi: 10.31838/jcr.07.07.146

[4]

NAKAMURA M, TAKENO K. Green base station using robust solar system and high performance lithium ion battery for next generation wireless network (5G) and against mega disaster[C]//IEEE. 2018 International Power Electronics Conference (IPEC-Niigata 2018 -ECCE Asia). Niigata, Japan, 2018: 201-206.

[5]

CHOUDHARI V G, DHOBLE D A S, SATHE T M. A review on effect of heat generation and various thermal management systems for lithium ion battery used for electric vehicle[J]. Journal of Energy Storage, 2020, 32: 101729. doi: 10.1016/j.est.2020.101729

[6]

DEPCIK C, CASSADY T, COLLICOTT B, et al. Comparison of lithium ion batteries, hydrogen fueled combustion engines, and a hydrogen fuel cell in powering a small unmanned aerial vehicle[J]. Energy Conversion and Management, 2020, 207: 112514. doi: 10.1016/j.enconman.2020.112514

[7]

LI P F, BASHIRULLAH R. A wireless power interface for rechargeable battery operated medical implants[J]. IEEE Transactions on Circuits and Systems II: Express Briefs, 2007, 54(10): 912-916. doi: 10.1109/TCSII.2007.901613

[8]

CHEN T M, JIN Y, LV H, et al. Applications of lithium-ion batteries in grid-scale energy storage systems[J]. Transactions of Tianjin University, 2020, 26(3): 208-217. doi: 10.1007/s12209-020-00236-w

[9]

ZHENG Y, SONG W, MO W T, et al. Lithium fluoride recovery from cathode material of spent lithium-ion battery[J]. RSC Advances, 2018, 8(16): 8990-8998. doi: 10.1039/C8RA00061A

[10]

东莞市钜大电子有限公司. 2020年全球动力锂离子电池行业市场现状及发展前景分析[EB/OL]. (2020-05-02) [2020-09-20]. http://www.juda.cn/news/134330.html.

[11]

FAN E S, LI L, WANG Z P, et al. Sustainable recycling technology for Li-ion batteries and beyond: Challenges and future prospects[J]. Chemical Reviews, 2020, 120(14): 7020-7063. doi: 10.1021/acs.chemrev.9b00535

[12]

YUAN Y, YU H X, CHENG X, et al. Preparation of TiNb₆O₁₇ nanospheres as high-performance anode candidates for lithium-ion storage[J]. Chemical Engineering Journal, 2019, 374: 937-946. doi: 10.1016/j.cej.2019.05.225

[13]

DIEKMANN J, HANISCH C, FROBÖSE L, et al. Ecological recycling of lithium-ion batteries from electric vehicles with focus on mechanical processes[J]. Journal of the Electrochemical Society, 2016, 164(1): A6184-A6191.

[14]

MESHRAM P, PANDEY B D, MANKHAND T R. Extraction of lithium from primary and secondary sources by pre-treatment, leaching and separation: A comprehensive review[J]. Hydrometallurgy, 2014, 150: 192-208. doi: 10.1016/j.hydromet.2014.10.012

[15]

TEDJAR F. Approach of “Electrodes to Electrodes”: Challenges for recycling advanced lithium-ion batteries for e-mobility[C]//IOP Publishing. 2014 ECS Meeting Abstracts. Como, Italy, 2014: 396.

[16]

LAROUCHE F, TEDJAR F, AMOUZEGAR K, et al. Progress and status of hydrometallurgical and direct recycling of Li-ion batteries and beyond[J]. Materials, 2020, 13(3): 801. doi: 10.3390/ma13030801

[17]

KATWALA A. The spiralling environmental cost of our lithium battery addiction[EB/OL]. [2018-08-05]. https://www.wired.co.uk/article/lithium-batteries-environment-impact, 2018.

[18]

LARCHER D, TARASCON J M. Towards greener and more sustainable batteries for electrical energy storage[J]. Nature Chemistry, 2015, 7(1): 19-29. doi: 10.1038/nchem.2085

[19]

LIANG S S, YAN W Q, WU X, et al. Gel polymer electrolytes for lithium ion batteries: Fabrication, characterization and performance[J]. Solid State Ionics, 2018, 318: 2-18. doi: 10.1016/j.ssi.2017.12.023

[20]

LIU Y J, ZHANG Z Q, FU Y B, et al. Investigation the electrochemical performance of Li_1.2Ni_0.2Mn_0.6O₂ cathode material with ZnAl₂O₄ coating for lithium ion batteries[J]. Journal of Alloys and Compounds, 2016, 685: 523-532. doi: 10.1016/j.jallcom.2016.05.329

[21]

HARPER G, SOMMERVILLE R, KENDRICK E, et al. Recycling lithium-ion batteries from electric vehicles[J]. Nature, 2019, 575(7781): 75-86. doi: 10.1038/s41586-019-1682-5

[22]

欧秀芹, 孙新华, 程耀丽. 废锂离子电池的综合处理方法[J]. 天津化工, 2002, 16(4): 35-36. doi: 10.3969/j.issn.1008-1267.2002.04.018

[23]

ZHANG W, XU C, HE W, et al. A review on management of spent lithium ion batteries and strategy for resource recycling of all components from them[J]. Waste Management & Research, 2018, 36(2): 99-112.

[24]

ZHANG X, LI L, FAN E, et al. Toward sustainable and systematic recycling of spent rechargeable batteries[J]. Chemical Society Reviews, 2018, 47(19): 7239-7302. doi: 10.1039/C8CS00297E

[25]

HUANG B, PAN Z F, SU X Y, et al. Recycling of lithium-ion batteries: Recent advances and perspectives[J]. Journal of Power Sources, 2018, 399: 274-286. doi: 10.1016/j.jpowsour.2018.07.116

[26]

KIM H, JANG Y C, HWANG Y, et al. End-of-life batteries management and material flow analysis in South Korea[J]. Frontiers of Environmental Science & Engineering, 2018, 12(3): 1-13.

[27]

BOXALL N J, KING S, CHENG K Y, et al. Urban mining of lithium-ion batteries in Australia: Current state and future trends[J]. Minerals Engineering, 2018, 128: 45-55. doi: 10.1016/j.mineng.2018.08.030

[28]

ZENG X L, LI J H, SINGH N. Recycling of spent lithium-ion battery: A critical review[J]. Critical Reviews in Environmental Science and Technology, 2014, 44(10): 1129-1165. doi: 10.1080/10643389.2013.763578

[29]

GUO Q S, SUN D W, CHENG J H, et al. Microwave processing techniques and their recent applications in the food industry[J]. Trends in Food Science & Technology, 2017, 67: 236-247.

[30]

ZHANG F, ZHOU T, LIU Y, et al. Microwave synthesis and actuation of shape memory polycaprolactone foams with high speed[J]. Scientific Reports, 2015, 5: 11152. doi: 10.1038/srep11152

[31]

BRODIE G. Applications of Microwave Heating in Agricultural and Forestry Related Industries[M]. Rijeka, Croatia: InTech, 2012: 45-78.

[32]

HUANG Y F, CHIUEH P T, LO S L. A review on microwave pyrolysis of lignocellulosic biomass[J]. Sustainable Environment Research, 2016, 26(3): 103-109. doi: 10.1016/j.serj.2016.04.012

[33]

SUN J, JIANG Z Y, WANG K, et al. Experimental study on microwave-SiC-assisted catalytic hydrogenation of phenol[J]. Energy & Fuels, 2019, 33(11): 11092-11100.

[34]

SUN J, WANG W L, LIU Z, et al. Recycling of waste printed circuit boards by microwave-induced pyrolysis and featured mechanical processing[J]. Industrial & Engineering Chemistry Research, 2011, 50(20): 11763-11769.

[35]

SUN J, WANG W L, YUE Q Y. Review on microwave-matter interaction fundamentals and efficient microwave-associated heating strategies[J]. Materials, 2016, 9(4): 231. doi: 10.3390/ma9040231

[36]

MISHRA R R, SHARMA A K. Microwave-material interaction phenomena: Heating mechanisms, challenges and opportunities in material processing[J]. Composites Part A: Applied Science and Manufacturing, 2016, 81: 78-97. doi: 10.1016/j.compositesa.2015.10.035

[37]

STUERGA D . Microwave-Material Interactions and Dielectric Properties, Key Ingredients for Mastery of Chemical Microwave Processes[M]. Weinhem: WILEY-VCH Verlag GmbH & Co, 2006.

[38]

ZHAO Y Z, LIU B G, ZHANG L B, et al. Microwave-absorbing properties of cathode material during reduction roasting for spent lithium-ion battery recycling[J]. Journal of Hazardous Materials, 2020, 384: 121487. doi: 10.1016/j.jhazmat.2019.121487

[39]

PINDAR S, DHAWAN N. Microwave processing of spent coin cells for recycling of metallic values[J]. Journal of Cleaner Production, 2021, 280: 124144. doi: 10.1016/j.jclepro.2020.124144

[40]

HE F, CHEN J, CHEN G, et al. Microwave dielectric properties and reduction behavior of low-grade pyrolusite[J]. JOM, 2019, 71(11): 3909-3914. doi: 10.1007/s11837-019-03522-8

[41]

LIU T, PANG Y, ZHU M, et al. Microporous Co@CoO nanoparticles with superior microwave absorption properties[J]. Nanoscale, 2014, 6(4): 2447-2454. doi: 10.1039/c3nr05238a

[42]

FARAG S, SOBHY A, AKYEL C, et al. Temperature profile prediction within selected materials heated by microwaves at 2.45GHz[J]. Applied Thermal Engineering, 2012, 36: 360-369. doi: 10.1016/j.applthermaleng.2011.10.049

[43]

GUPTA M, LEONG E W W. Microwaves and Metals[M]. John Wiley & Sons, 2008.

[44]

JILES D. Introduction to Magnetism and Magnetic Materials[M]. CRC Press, 2015.

[45]

GIERAS J F, PIECH Z J, TOMCZUK B. Linear Synchronous Motors: Transportation and Automation Systems[M]. CRC Press, 2016.

[46]

MENÉNDEZ J A, ARENILLAS A, FIDALGO B, et al. Microwave heating processes involving carbon materials[J]. Fuel Processing Technology, 2010, 91(1): 1-8. doi: 10.1016/j.fuproc.2009.08.021

[47]

MONSEF-MIRZAI P, RAVINDRAN M, MCWHINNIE W R, et al. Rapid microwave pyrolysis of coal: Methodology and examination of the residual and volatile phases[J]. Fuel, 1995, 74(1): 20-27. doi: 10.1016/0016-2361(94)P4325-V

[48]

EL HARFI K, MOKHLISSE A, CHANÂA M B, et al. Pyrolysis of the Moroccan (Tarfaya) oil shales under microwave irradiation[J]. Fuel, 2000, 79(7): 733-742. doi: 10.1016/S0016-2361(99)00209-4

[49]

FERNÁNDEZ Y, ARENILLAS A, DÍEZ M A, et al. Pyrolysis of glycerol over activated carbons for syngas production[J]. Journal of Analytical and Applied Pyrolysis, 2009, 84(2): 145-150. doi: 10.1016/j.jaap.2009.01.004

[50]

MENÉNDEZ J A, MENÉNDEZ E M, GARCÍA A, et al. Thermal treatment of active carbons: A comparison between microwave and electrical hating[J]. Journal of Microwave Power and Electromagnetic Energy, 1999, 34(3): 137-143. doi: 10.1080/08327823.1999.11688398

[51]

FIDALGO B, ARENILLAS A, MENÉNDEZ J A. Influence of porosity and surface groups on the catalytic activity of carbon materials for the microwave-assisted CO₂ reforming of CH₄[J]. Fuel, 2010, 89(12): 4002-4007. doi: 10.1016/j.fuel.2010.06.015

[52]

SUN J, WANG W L, YUE Q Y, et al. Review on microwave-metal discharges and their applications in energy and industrial processes[J]. Applied Energy, 2016, 175: 141-157. doi: 10.1016/j.apenergy.2016.04.091

[53]

DIAZ F, WANG Y, MOORTHY T, et al. Degradation mechanism of nickel-cobalt-aluminum (NCA) cathode material from spent lithium-ion batteries in microwave-assisted pyrolysis[J]. Metals, 2018, 8(8): 565. doi: 10.3390/met8080565

[54]

BAJPAI R, WAGNER H D. Fast growth of carbon nanotubes using a microwave oven[J]. Carbon, 2015, 82: 327-336. doi: 10.1016/j.carbon.2014.10.077

[55]

DIAZ F, FLERUS B, NAGRAJ S, et al. Comparative analysis about degradation mechanisms of printed circuit boards (PCBs) in slow and fast pyrolysis: The influence of heating speed[J]. Journal of Sustainable Metallurgy, 2018, 4(2): 205-221. doi: 10.1007/s40831-018-0163-7

[56]

NIE H, XU L, SONG D, et al. LiCoO₂: Recycling from spent batteries and regeneration with solid state synthesis[J]. Green Chemistry, 2015, 17(2): 1276-1280. doi: 10.1039/C4GC01951B

[57]

CHOUBEY P K, KIM M S, SRIVASTAVA R R, et al. Advance review on the exploitation of the prominent energy-storage element: Lithium. Part I: From mineral and brine resources[J]. Minerals Engineering, 2016, 89: 119-137. doi: 10.1016/j.mineng.2016.01.010

[58]

LI J H, SHI P X, WANG Z F, et al. A combined recovery process of metals in spent lithium-ion batteries[J]. Chemosphere, 2009, 77(8): 1132-1136. doi: 10.1016/j.chemosphere.2009.08.040

[59]

HE L P, SUN S Y, SONG X F, et al. Recovery of cathode materials and Al from spent lithium-ion batteries by ultrasonic cleaning[J]. Waste Management, 2015, 46: 523-528. doi: 10.1016/j.wasman.2015.08.035

[60]

ZENG X L, LI J H. Innovative application of ionic liquid to separate Al and cathode materials from spent high-power lithium-ion batteries[J]. Journal of Hazardous Materials, 2014, 271: 50-56. doi: 10.1016/j.jhazmat.2014.02.001

[61]

CHEN L, TANG X C, ZHANG Y, et al. Process for the recovery of cobalt oxalate from spent lithium-ion batteries[J]. Hydrometallurgy, 2011, 108(1/2): 80-86.

[62]

WANG M M, TAN Q Y, LIU L L, et al. Efficient separation of aluminum foil and cathode materials from spent lithium-ion batteries using a low-temperature molten salt[J]. ACS Sustainable Chemistry & Engineering, 2019, 7(9): 8287-8294.

[63]

SUN L, QIU K Q. Vacuum pyrolysis and hydrometallurgical process for the recovery of valuable metals from spent lithium-ion batteries[J]. Journal of Hazardous Materials, 2011, 194: 378-384. doi: 10.1016/j.jhazmat.2011.07.114

[64]

ZHANG T, HE Y Q, GE L H, et al. Characteristics of wet and dry crushing methods in the recycling process of spent lithium-ion batteries[J]. Journal of Power Sources, 2013, 240: 766-771. doi: 10.1016/j.jpowsour.2013.05.009

[65]

汪永威, 赵光金, 朱莉娜, 等. 一种微波热解处理废旧锂电池的方法: CN103247837A[P]. 2013-08-14.

[66]

殷衡. 一种以等离子体技术回收三元电池正极材料的方法: CN108199107B[P]. 2020-02-18.

[67]

刘云建, 胡启阳, 李新海, 等. 从不合格锂离子蓄电池中直接回收钴酸锂[J]. 电源技术, 2006, 30(4): 308-310. doi: 10.3969/j.issn.1002-087X.2006.04.015

[68]

GEORGI-MASCHLER T, FRIEDRICH B, WEYHE R, et al. Development of a recycling process for Li-ion batteries[J]. Journal of Power Sources, 2012, 207: 173-182. doi: 10.1016/j.jpowsour.2012.01.152

[69]

LI J, WANG G X, XU Z M. Environmentally-friendly oxygen-free roasting/wet magnetic separation technology for in situ recycling cobalt, lithium carbonate and graphite from spent LiCoO₂/graphite lithium batteries[J]. Journal of Hazardous Materials, 2016, 302: 97-104. doi: 10.1016/j.jhazmat.2015.09.050

[70]

XIAO J F, LI J, XU Z M. Recycling metals from lithium ion battery by mechanical separation and vacuum metallurgy[J]. Journal of Hazardous Materials, 2017, 338: 124-131. doi: 10.1016/j.jhazmat.2017.05.024

[71]

FAN E S, LI L, LIN J, et al. Low-temperature molten-salt-assisted recovery of valuable metals from spent lithium-ion batteries[J]. ACS Sustainable Chemistry & Engineering, 2019, 7(19): 16144-16150.

[72]

HU J T, ZHANG J L, LI H X, et al. A promising approach for the recovery of high value-added metals from spent lithium-ion batteries[J]. Journal of Power Sources, 2017, 351: 192-199. doi: 10.1016/j.jpowsour.2017.03.093

[73]

LIU P C, XIAO L, CHEN Y F, et al. Recovering valuable metals from LiNi_xCo_yMn_1-_x_-_yO₂ cathode materials of spent lithium ion batteries via a combination of reduction roasting and stepwise leaching[J]. Journal of Alloys and Compounds, 2019, 783: 743-752. doi: 10.1016/j.jallcom.2018.12.226

[74]

LI J H, LI X H, HU Q Y, et al. Study of extraction and purification of Ni, Co and Mn from spent battery material[J]. Hydrometallurgy, 2009, 99(1/2): 7-12.

[75]

JOULIÉ M, LAUCOURNET R, BILLY E. Hydrometallurgical process for the recovery of high value metals from spent lithium nickel cobalt aluminum oxide based lithium-ion batteries[J]. Journal of Power Sources, 2014, 247: 551-555. doi: 10.1016/j.jpowsour.2013.08.128

[76]

ZHANG P W, YOKOYAMA T, ITABASHI O, et al. Hydrometallurgical process for recovery of metal values from spent lithium-ion secondary batteries[J]. Hydrometallurgy, 1998, 47(2/3): 259-271.

[77]

LI L, LU J, REN Y, et al. Ascorbic-acid-assisted recovery of cobalt and lithium from spent Li-ion batteries[J]. Journal of Power Sources, 2012, 218: 21-27. doi: 10.1016/j.jpowsour.2012.06.068

[78]

LI L, GE J, CHEN R J, et al. Environmental friendly leaching reagent for cobalt and lithium recovery from spent lithium-ion batteries[J]. Waste Management, 2010, 30(12): 2615-2621. doi: 10.1016/j.wasman.2010.08.008

[79]

LI L, ZHAI L Y, ZHANG X X, et al. Recovery of valuable metals from spent lithium-ion batteries by ultrasonic-assisted leaching process[J]. Journal of Power Sources, 2014, 262: 380-385. doi: 10.1016/j.jpowsour.2014.04.013

[80]

LI L, GE J, WU F, et al. Recovery of cobalt and lithium from spent lithium ion batteries using organic citric acid as leachant[J]. Journal of Hazardous Materials, 2010, 176(1/2/3): 288-293.

[81]

MISHRA D, KIM D J, RALPH D E, et al. Bioleaching of metals from spent lithium ion secondary batteries using Acidithiobacillus ferrooxidans[J]. Waste Management, 2008, 28(2): 333-338. doi: 10.1016/j.wasman.2007.01.010

[82]

XIN B P, ZHANG D, ZHANG X, et al. Bioleaching mechanism of Co and Li from spent lithium-ion battery by the mixed culture of acidophilic sulfur-oxidizing and iron-oxidizing bacteria[J]. Bioresource Technology, 2009, 100(24): 6163-6169. doi: 10.1016/j.biortech.2009.06.086

[83]

ZENG G S, DENG X R, LUO S L, et al. A copper-catalyzed bioleaching process for enhancement of cobalt dissolution from spent lithium-ion batteries[J]. Journal of Hazardous Materials, 2012, 199/200: 164-169. doi: 10.1016/j.jhazmat.2011.10.063

[84]

ZHAO Y Z, LIU B G, ZHANG L B, et al. Microwave pyrolysis of macadamia shells for efficiently recycling lithium from spent lithium-ion batteries[J]. Journal of Hazardous Materials, 2020, 396: 122740. doi: 10.1016/j.jhazmat.2020.122740

[85]

YIXIN H, CHUNPENG L. Microwave-assisted carbothermic reduction of ilmenite[J]. Acta Metallurgica Sinica (English Letters), 2009, 9(3): 164-170.

[86]

RU J J, HUA Y X, WANG D. Preparation and characterisation of TiN by microwave-assisted carbothermic reduction-nitridation in air atmosphere[J]. Advances in Applied Ceramics, 2017, 116(8): 468-476. doi: 10.1080/17436753.2017.1357292

[87]

CHE X K, SU X Z, CHI R A, et al. Microwave assisted atmospheric acid leaching of nickel from laterite ore[J]. Rare Metals, 2010, 29(3): 327-332. doi: 10.1007/s12598-010-0058-7

[88]

SAMOUHOS M, TAXIARCHOU M, HUTCHEON R, et al. Microwave reduction of a nickeliferous laterite ore[J]. Minerals Engineering, 2012, 34: 19-29. doi: 10.1016/j.mineng.2012.04.005

[89]

CHANG Y F, ZHAI X J, FU Y, et al. Phase transformation in reductive roasting of laterite ore with microwave heating[J]. Transactions of Nonferrous Metals Society of China, 2008, 18(4): 969-973. doi: 10.1016/S1003-6326(08)60167-3

[90]

KRUESI P R, FRAHM JR V H. Process for the recovery of nickel, cobalt and manganese from their oxides and silicates: U.S. Patent No. 4, 311, 520 [P]. 1982-01-19.

[91]

ZHAO Y, GAO J M, YUE Y, et al. Extraction and separation of nickel and cobalt from saprolite laterite ore by microwave-assisted hydrothermal leaching and chemical deposition[J]. International Journal of Minerals, Metallurgy, and Materials, 2013, 20(7): 612-619. doi: 10.1007/s12613-013-0774-8

[92]

LIU X X, ZHANG Z Y, WU Y P. Absorption properties of carbon black/silicon carbide microwave absorbers[J]. Composites Part B: Engineering, 2011, 42(2): 326-329. doi: 10.1016/j.compositesb.2010.11.009

[93]

PINDAR S, DHAWAN N. Recycling of mixed discarded lithium-ion batteries via microwave processing route[J]. Sustainable Materials and Technologies, 2020, 25: e00157. doi: 10.1016/j.susmat.2020.e00157

[94]

SUNIL S R, DHAWAN N. Thermal processing of spent Li-ion batteries for extraction of lithium and cobalt-manganese values[J]. Transactions of the Indian Institute of Metals, 2019, 72(12): 3035-3044. doi: 10.1007/s12666-019-01769-y

[95]

PINDAR S, DHAWAN N. Carbothermal reduction of spent mobile phones batteries for the recovery of lithium, cobalt, and manganese values[J]. JOM, 2019, 71(12): 4483-4491. doi: 10.1007/s11837-019-03799-9

[96]

PINDAR S, DHAWAN N. Comparison of microwave and conventional indigenous carbothermal reduction for recycling of discarded lithium-ion batteries[J]. Transactions of the Indian Institute of Metals, 2020, 73(8): 2041-2051. doi: 10.1007/s12666-020-01956-2

[97]

SUNIL S R, VISHVAKARMA S, BARNWAL A, et al. Processing of spent Li-ion batteries for recovery of cobalt and lithium values[J]. JOM, 2019, 71(12): 4659-4665. doi: 10.1007/s11837-019-03540-6

[98]

NATARAJAN S, ANANTHARAJ S, TAYADE R J, et al. Recovered spinel MnCo₂O₄ from spent lithium-ion batteries for enhanced electrocatalytic oxygen evolution in alkaline medium[J]. Dalton Transaction, 2017, 46(41): 14382-14392. doi: 10.1039/C7DT02613G

[99]

XI G X, ZHAO T T, WANG L, et al. Effect of doping rare earths on magnetostriction characteristics of CoFe₂O₄ prepared from spent Li-ion batteries[J]. Physica B: Condensed Matter, 2018, 534: 76-82. doi: 10.1016/j.physb.2018.01.036

[100]

MOURA M N, BARRADA R V, ALMEIDA J R, et al. Synthesis, characterization and photocatalytic properties of nanostructured CoFe₂O₄ recycled from spent Li-ion batteries[J]. Chemosphere, 2017, 182: 339-347. doi: 10.1016/j.chemosphere.2017.05.036

[101]

FERREIRA D A, PRADOS L M Z, MAJUSTE D, et al. Hydrometallurgical separation of aluminium, cobalt, copper and lithium from spent Li-ion batteries[J]. Journal of Power Sources, 2009, 187(1): 238-246. doi: 10.1016/j.jpowsour.2008.10.077

[102]

JHA M K, KUMARI A, JHA A K, et al. Recovery of lithium and cobalt from waste lithium ion batteries of mobile phone[J]. Waste Management, 2013, 33(9): 1890-1897. doi: 10.1016/j.wasman.2013.05.008

[103]

LI L, CHEN R J, SUN F, et al. Preparation of LiCoO₂ films from spent lithium-ion batteries by a combined recycling process[J]. Hydrometallurgy, 2011, 108(3/4): 220-225.

[104]

FAN E S, LI L, ZHANG X X, et al. Selective recovery of Li and Fe from spent lithium-ion batteries by an environmentally friendly mechanochemical approach[J]. ACS Sustainable Chemistry & Engineering, 2018, 6(8): 11029-11035.

[105]

WANG M M, ZHANG C C, ZHANG F S. An environmental benign process for cobalt and lithium recovery from spent lithium-ion batteries by mechanochemical approach[J]. Waste Management, 2016, 51: 239-244. doi: 10.1016/j.wasman.2016.03.006

[106]

LI J G, ZHAO R S, HE X M, et al. Preparation of LiCoO₂ cathode materials from spent lithium-ion batteries[J]. Ionics, 2009, 15(1): 111-113. doi: 10.1007/s11581-008-0238-8

[107]

PATIL D, CHIKKAMATH S, KENY S, et al. Rapid dissolution and recovery of Li and Co from spent LiCoO₂ using mild organic acids under microwave irradiation[J]. Journal of Environmental Management, 2020, 256: 109935. doi: 10.1016/j.jenvman.2019.109935

[108]

ZOU H Y, GRATZ E, APELIAN D, et al. A novel method to recycle mixed cathode materials for lithium ion batteries[J]. Green Chemistry, 2013, 15(5): 1183. doi: 10.1039/c3gc40182k

[109]

SA Q N, GRATZ E, HEELAN J A, et al. Synthesis of diverse LiNi_xMn_yCo_zO₂ cathode materials from lithium ion battery recovery stream[J]. Journal of Sustainable Metallurgy, 2016, 2(3): 248-256. doi: 10.1007/s40831-016-0052-x

[110]

SHI Y, CHEN G, LIU F, et al. Resolving the compositional and structural defects of degraded LiNi_xCo_yMn_zO₂ particles to directly regenerate high-performance lithium-ion battery cathodes[J]. ACS Energy Letters, 2018, 3(7): 1683-1692. doi: 10.1021/acsenergylett.8b00833

[111]

ZHANG X H, CAO H B, XIE Y B, et al. A closed-loop process for recycling LiNi_1/3Co_1/3Mn_1/3O₂ from the cathode scraps of lithium-ion batteries: Process optimization and kinetics analysis[J]. Separation and Purification Technology, 2015, 150: 186-195. doi: 10.1016/j.seppur.2015.07.003

[112]

HE L P, SUN S Y, SONG X F, et al. Leaching process for recovering valuable metals from the LiNi_1/3Co_1/3Mn_1/3O₂ cathode of lithium-ion batteries[J]. Waste Management, 2017, 64: 171-181. doi: 10.1016/j.wasman.2017.02.011

[113]

MESHRAM P, PANDEY B D, MANKHAND T R. Recovery of valuable metals from cathodic active material of spent lithium ion batteries: Leaching and kinetic aspects[J]. Waste Management, 2015, 45: 306-313. doi: 10.1016/j.wasman.2015.05.027

[114]

GOLMOHAMMADZADEH R, RASHCHI F, VAHIDI E. Recovery of lithium and cobalt from spent lithium-ion batteries using organic acids: Process optimization and kinetic aspects[J]. Waste Management, 2017, 64: 244-254. doi: 10.1016/j.wasman.2017.03.037

[115]

FU Y P, HE Y Q, YANG Y, et al. Microwave reduction enhanced leaching of valuable metals from spent lithium-ion batteries[J]. Journal of Alloys and Compounds, 2020, 832: 154920. doi: 10.1016/j.jallcom.2020.154920

[116]

LI L, BIAN Y F, ZHANG X X, et al. Economical recycling process for spent lithium-ion batteries and macro- and micro-scale mechanistic study[J]. Journal of Power Sources, 2018, 377: 70-79. doi: 10.1016/j.jpowsour.2017.12.006

[117]

LANNOO S, VILAS-BOAS A, SADEGHI S M, et al. An environmentally friendly closed loop process to recycle raw materials from spent alkaline batteries[J]. Journal of Cleaner Production, 2019, 236: 117612. doi: 10.1016/j.jclepro.2019.117612

[118]

KARIMI G R, ROWSON N A, HEWITT C J. Bioleaching of copper via iron oxidation from chalcopyrite at elevated temperatures[J]. Food and Bioproducts Processing, 2010, 88(1): 21-25. doi: 10.1016/j.fbp.2009.06.005

[119]

SMITH S L, GRAIL B M, JOHNSON D B. Reductive bioprocessing of cobalt-bearing limonitic laterites[J]. Minerals Engineering, 2017, 106: 86-90. doi: 10.1016/j.mineng.2016.09.009

[120]

HOREH N B, MOUSAVI S M, SHOJAOSADATI S A. Bioleaching of valuable metals from spent lithium-ion mobile phone batteries using Aspergillus Niger[J]. Journal of Power Sources, 2016, 320: 257-266. doi: 10.1016/j.jpowsour.2016.04.104

[121]

XIN Y Y, GUO X M, CHEN S, et al. Bioleaching of valuable metals Li, Co, Ni and Mn from spent electric vehicle Li-ion batteries for the purpose of recovery[J]. Journal of Cleaner Production, 2016, 116: 249-258. doi: 10.1016/j.jclepro.2016.01.001

[122]

POLLMANN K, RAFF J, MERROUN M, et al. Metal binding by bacteria from uranium mining waste piles and its technological applications[J]. Biotechnology Advances, 2006, 24(1): 58-68. doi: 10.1016/j.biotechadv.2005.06.002

[123]

MACASKIE L E, MIKHEENKO I P, YONG P, et al. Today's wastes, tomorrow's materials for environmental protection[J]. Hydrometallurgy, 2010, 104(3/4): 483-487.

[124]

YEMIŞ O, MAZZA G. Acid-catalyzed conversion of xylose, xylan and straw into furfural by microwave-assisted reaction[J]. Bioresource Technology, 2011, 102(15): 7371-7378. doi: 10.1016/j.biortech.2011.04.050

[125]

RAMASAMY S, MOGHTADERI B. Dielectric properties of typical Australian wood-based biomass materials at microwave frequency[J]. Energy & Fuels, 2010, 24(8): 4534-4548.

[126]

SAIT H H, SALEMA A A. Microwave dielectric characterization of Saudi Arabian date palm biomass during pyrolysis and at industrial frequencies[J]. Fuel, 2015, 161: 239-247. doi: 10.1016/j.fuel.2015.08.058

[127]

TATEISHI K, DU BOULAY D, ISHIZAWA N, et al. Structural disorder along the lithium diffusion pathway in cubically stabilized lithium manganese spinel II. Molecular dynamics calculation[J]. Journal of Solid State Chemistry, 2003, 174(1): 175-181. doi: 10.1016/S0022-4596(03)00207-X

[128]

YOON W S, IANNOPOLLO S, GREY C P, et al. Local structure and cation ordering in O₃ lithium nickel manganese oxides with stoichiometry Li[Ni_xMn_(2–_x_)/3Li_(1–2_x_)/3]O₂[J]. Electrochemical and Solid-State Letters, 2004, 7(7): A167. doi: 10.1149/1.1737711

[129]

GADJOV H, GOROVA M, KOTZEVA V, et al. LiMn₂O₄ prepared by different methods at identical thermal treatment conditions: structural, morphological and electrochemical characteristics[J]. Journal of Power Sources, 2004, 134(1): 110-117. doi: 10.1016/j.jpowsour.2004.03.027

[130]

RODRÍGUEZ-CARVAJAL J, ROUSSE G, MASQUELIER C, et al. Electronic crystallization in a lithium battery material: Columnar ordering of electrons and holes in the Spinel LiMn₂O₄[J]. Physical Review Letters, 1998, 81(21): 4660. doi: 10.1103/PhysRevLett.81.4660

[131]

GILBERT J A, SHKROB I A, ABRAHAM D P. Transition metal dissolution, ion migration, electrocatalytic reduction and capacity loss in lithium-ion full cells[J]. Journal of the Electrochemical Society, 2017, 164(2): A389-A399. doi: 10.1149/2.1111702jes

[132]

MENG X Q, HAO J, CAO H B, et al. Recycling of LiNi_1/3Co_1/3Mn_1/3O₂ cathode materials from spent lithium-ion batteries using mechanochemical activation and solid-state sintering[J]. Waste Management, 2019, 84: 54-63. doi: 10.1016/j.wasman.2018.11.034

[133]

张维民, 张娜, 张铁柱, 等. 废弃电池回收再生制备锂电池三元正极材料的方法: CN110265659A[P]. 2019-09-20.

[134]

刘静静, 仇卫华, 赵海雷, 等. 锂离子电池用层状LiMnO₂基正极材料的研究进展[J]. 硅酸盐学报, 2005, 33(9): 1127-1132. doi: 10.3321/j.issn:0454-5648.2005.09.016

[135]

SHI Y, ZHANG M H, MENG Y S, et al. Ambient-pressure relithiation of degraded Li_xNi_0.5Co_0.2Mn_0.3O₂ (0<x<1) via eutectic solutions for direct regeneration of lithium-ion battery cathodes[J]. Advanced Energy Materials, 2019, 9(20): 1900454. doi: 10.1002/aenm.201900454

[136]

KIM D S, SOHN J S, LEE C K, et al. Simultaneous separation and renovation of lithium cobalt oxide from the cathode of spent lithium ion rechargeable batteries[J]. Journal of Power Sources, 2004, 132(1/2): 145-149.

[137]

CONTESTABILE M, PANERO S, SCROSATI B. A laboratory-scale lithium-ion battery recycling process[J]. Journal of Power Sources, 2001, 92(1/2): 65-69.

[138]

LIU Y J, HU Q Y, LI X H, et al. Recycle and synthesis of LiCoO₂ from incisors bound of Li-ion batteries[J]. Transactions of Nonferrous Metals Society of China, 2006, 16(4): 956-959. doi: 10.1016/S1003-6326(06)60359-2

[139]

SA Q N, GRATZ E, HE M N, et al. Synthesis of high performance LiNi_1/3Mn_1/3Co_1/3O₂ from lithium ion battery recovery stream[J]. Journal of Power Sources, 2015, 282: 140-145. doi: 10.1016/j.jpowsour.2015.02.046

[140]

LEE C K, RHEE K I. Preparation of LiCoO₂ from spent lithium-ion batteries[J]. Journal of Power Sources, 2002, 109(1): 17-21. doi: 10.1016/S0378-7753(02)00037-X

[141]

LEE C K, RHEE K I. Reductive leaching of cathodic active materials from lithium ion battery wastes[J]. Hydrometallurgy, 2003, 68(1/2/3): 5-10.

[142]

BALAJI S, MUTHARASU D, SANKARA SUBRAMANIAN N, et al. A review on microwave synthesis of electrode materials for lithium-ion batteries[J]. Ionics, 2009, 15(6): 765-777. doi: 10.1007/s11581-009-0350-4

[143]

LI J, WANG Y, WANG L H, et al. A facile recycling and regeneration process for spent LiFePO₄ batteries[J]. Journal of Materials Science: Materials in Electronics, 2019, 30(15): 14580-14588. doi: 10.1007/s10854-019-01830-y

[144]

LI X L, ZHANG J, SONG D W, et al. Direct regeneration of recycled cathode material mixture from scrapped LiFePO₄ batteries[J]. Journal of Power Sources, 2017, 345: 78-84. doi: 10.1016/j.jpowsour.2017.01.118

[145]

BAO S J, LIANG Y Y, LI H L. Synthesis and electrochemical properties of LiMn₂O₄ by microwave-assisted Sol-gel method[J]. Materials Letters, 2005, 59(28): 3761-3765. doi: 10.1016/j.matlet.2005.07.012

[146]

TANG X, WANG R, REN Y F, et al. Effective regeneration of scrapped LiFePO₄ material from spent lithium-ion batteries[J]. Journal of Materials Science, 2020, 55(27): 13036-13048. doi: 10.1007/s10853-020-04907-w

[147]

YAN H W, HUANG X J, LI H, et al. Electrochemical study on LiCoO₂ synthesized by microwave energy[J]. Solid State Ionics, 1998, 113-115: 11-15.

[148]

ELUMALAI P, VASAN H N, MUNICHANDRAIAH N. Microwave synthesis and electrochemical properties of LiCo₁₋_xM_xO₂ (M = Al and Mg) cathodes for Li-ion rechargeable batteries[J]. Journal of Power Sources, 2004, 125(1): 77-84. doi: 10.1016/S0378-7753(03)00815-2

[149]

LIU H X, HU C, ZHU X J, et al. Solid chemical reaction in microwave and millimeter-wave fields for the syntheses of LiMn₂O₄ compound[J]. Materials Chemistry and Physics, 2004, 88(2/3): 290-294.

[150]

FU Y P, LIN C H, SU Y H, et al. Electrochemical properties of LiMn₂O₄ synthesized by the microwave-induced combustion method[J]. Ceramics International, 2004, 30(7): 1953-1959. doi: 10.1016/j.ceramint.2003.12.183

[151]

CUI T, HUA N, HAN Y, et al. Preparation and electrochemical properties of LiMn₂O₄ by a rheological-phase-assisted microwave synthesis method[J]. Inorganic Materials, 2008, 44(5): 542-548. doi: 10.1134/S002016850805021X

[152]

HIGUCHI M, KATAYAMA K, AZUMA Y, et al. Synthesis of LiFePO₄ cathode material by microwave processing[J]. Journal of Power Sources, 2003, 119-121: 258-261.

[153]

LI J, JIN Y L, ZHANG X G, et al. Microwave solid-state synthesis of spinel Li₄Ti₅O₁₂ nanocrystallites as anode material for lithium-ion batteries[J]. Solid State Ionics, 2007, 178(29/30): 1590-1594.

[154]

FU Y P, SU Y H, WU S H, et al. LiMn₂₋_yM_yO₄ (M = Cr, Co) cathode materials synthesized by the microwave-induced combustion for lithium ion batteries[J]. Journal of Alloys and Compounds, 2006, 426(1/2): 228-234.

[155]

FU Y P, SU Y H, LIN C H. Comparison of microwave-induced combustion and solid-state reaction for synthesis of LiMn₂₋_xCr_xO₄ powders and their electrochemical properties[J]. Solid State Ionics, 2004, 166(1/2): 137-146.

[156]

LEE K S, MYUNG S T, PRAKASH J, et al. Optimization of microwave synthesis of Li[Ni_0.4Co_0.2Mn_0.4]O₂ as a positive electrode material for lithium batteries[J]. Electrochimica Acta, 2008, 53(7): 3065-3074. doi: 10.1016/j.electacta.2007.11.042

[157]

赵新兵, 周斌, 曹高劭, 等. 一种从磷酸铁锂废旧电池中回收制备磷酸铁锂的方法: CN102751548A[P]. 2012-10-24.

[158]

LI F X, QIU W H, HU H Y, et al. Electrochemical performance of LiFePO₄ synthesized by microwave processing as lithium battery cathode[J]. Chinese Journal of Power Sources, 2005, 29(6): 346.

[159]

AMINE K. Olivine LiCoPO₄ as 4.8 V electrode material for lithium batteries[J]. Electrochemical and Solid-State Letters, 1999, 3(4): 178. doi: 10.1149/1.1390994

[160]

OKADA S, SAWA S, EGASHIRA M, et al. Cathode properties of phospho-olivine LiMPO₄ for lithium secondary batteries[J]. Journal of Power Sources, 2001, 97-98: 430-432. doi: 10.1016/S0378-7753(01)00631-0

[161]

LLORIS J M, PÉREZ VICENTE C, TIRADO J L. Improvement of the electrochemical performance of LiCoPO₄ 5 V material using a novel synthesis procedure[J]. Electrochemical and Solid-State Letters, 2002, 5(10): A234. doi: 10.1149/1.1507941

[162]

LUDWIG J, MARINO C, HAERING D, et al. Morphology-controlled microwave-assisted solvothermal synthesis of high-performance LiCoPO₄ as a high-voltage cathode material for Li-ion batteries[J]. Journal of Power Sources, 2017, 342: 214-223. doi: 10.1016/j.jpowsour.2016.12.059

[163]

LUDWIG J, GEPRÄGS S, NORDLUND D, et al. Co₁₁Li[(OH)₅O][(PO₃OH)(PO₄)₅], a lithium-stabilized, mixed-valent cobalt(II, III) hydroxide phosphate framework[J]. Inorganic Chemistry, 2017, 56(18): 10950-10961. doi: 10.1021/acs.inorgchem.7b01152

[164]

ZAINI M A A, KAMARUDDIN M J. Critical issues in microwave-assisted activated carbon preparation[J]. Journal of Analytical and Applied Pyrolysis, 2013, 101: 238-241. doi: 10.1016/j.jaap.2013.02.003

[165]

CHATTERJEE S, BASAK T, DAS S K. Microwave driven convection in a rotating cylindrical cavity: A numerical study[J]. Journal of Food Engineering, 2007, 79(4): 1269-1279. doi: 10.1016/j.jfoodeng.2006.04.039

[166]

DATTA A K, HU W. Quality optimization of dielectric heating processes[J]. Food Technology, 1992, 46(12): 53-56.

[167]

ROUSSY G, JASSM S, THIEBAUT J M T. Modeling of a fluidized bed irradiatel by a single or a Mult1Mode electric microwave field distribution[J]. Journal of Microwave Power and Electromagnetic Energy, 1995, 30(3): 178-187. doi: 10.1080/08327823.1995.11688274

[168]

BASAK T, AYAPPA K G. Role of length scales on microwave thawing dynamics in 2D cylinders[J]. International Journal of Heat and Mass Transfer, 2002, 45(23): 4543-4559. doi: 10.1016/S0017-9310(02)00171-0

[169]

CHA-UM W, RATTANADECHO P, PAKDEE W. Experimental and numerical analysis of microwave heating of water and oil using a rectangular wave guide: Influence of sample sizes, positions, and microwave power[J]. Food and Bioprocess Technology, 2011, 4(4): 544-558. doi: 10.1007/s11947-009-0187-x

[170]

CHA-UM W, RATTANADECHO P, PAKDEE W. Experimental analysis of microwave heating of dielectric materials using a rectangular wave guide (MODE: TE10) (Case study: Water layer and saturated porous medium)[J]. Experimental Thermal and Fluid Science, 2009, 33(3): 472-481. doi: 10.1016/j.expthermflusci.2008.11.008

[171]

MORIWAKI S, MACHIDA M, TATSUMOTO H, et al. A study on thermal runaway of poly(vinyl chloride) by microwave irradiation[J]. Journal of Analytical and Applied Pyrolysis, 2006, 76(1/2): 238-242.

[172]

GUPTA N, MIDHA V, BALAKOTAIAH V, et al. Bifurcation analysis of thermal runaway in microwave heating of ceramics[J]. Journal of the Electrochemical Society, 1999, 146(12): 4659-4665. doi: 10.1149/1.1392690

[173]

KRIEGSMANN G A. Thermal runaway in microwave heated ceramics: A one-dimensional model[J]. Journal of Applied Physics, 1992, 71(4): 1960-1966. doi: 10.1063/1.351191

[174]

VRIEZINGA C A, SÁNCHEZ-PEDREÑO S, GRASMAN J. Thermal runaway in microwave heating: A mathematical analysis[J]. Applied Mathematical Modelling, 2002, 26(11): 1029-1038. doi: 10.1016/S0307-904X(02)00058-6

[175]

LIU B. The microwave heating of two-dimensional slabs with small Arrhenius absorptivity[J]. IMA Journal of Applied Mathematics, 1999, 62(2): 137-166. doi: 10.1093/imamat/62.2.137

[176]

ROUSSY G, BENNANI A, THIEBAUT J M. Temperature runaway of microwave irradiated materials[J]. Journal of Applied Physics, 1987, 62(4): 1167-1170. doi: 10.1063/1.339666